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Related article: 4. In our present assay processes alkali metrical titrations are in most
cases prescribed for determination of the several alkaloids. Results of
such titration are not always satisfactory. Query. Is there not some other
way of making determinations of some of the alkaloids ? A paper recently
published by Dr. Heikel Gunnar has revived interest in the use of Mayer's
reagent, once extensively used, but discarded of late years as lacking in
exactness. Dr. Gunnar adds to the solution containing an alkaloid an
excess of Mayer's reagent, and then determines the excess of mercury by
titration with silver nitrate after addition of potassium cyanide. He claims
a degree of exactness for his results that should make it available for the
purposes of drug standardization. It may prove in Buy Norvasc Online the case of certain
drags to afford the most expeditious procedure. Even if it be not adopted
as the official method of determining any alkaloid, it may at least serve to
confirm the result of alkalimetrical titration where there is doubt regarding
the identity of the alkaloid extracted. In case at least of colchicine it
furnishes certainly the only titration method as yet known.
OPIUM ASSAY.
The lime assay has still warm advocates, Buy Norvasc Online and it commends itself Buy Norvasc Online by its
rapidity and by the exceptional purity possible of the morphine which it
extracts. However, the process involves the principle of the aliquot part,
with an inevitable uncertainty about the aliquot, and hence will practically
not find favor with the new committee.
Our present assay method is satisfactory, but may be improved in sev-
eral particulars. The two filters on which the morphjne is collected
should be of exactly equal weight [or else the difference in weight, which
Digitized by
Google
826 MINUTES OF THE SECTION ON SCIENTIFIC PAPERS.
should not exceed ten milligrams, should be marked plainly on the outer
(heavier) filter, and taken into account in the weighing of the morphine],
and the morphine should be weighed after drying on the inner filter, with
the outer used as counterpoise. It is not necessary to pass the ether
through the filter. It should be decanted into a small beaker (to make
sure that no morphine crystals go with it), and then rejected, using
afterwards three portions at least of 15 Cc. each to complete the removal
of narcotine, Buy Norvasc Online etc., each portion being decanted into the beaker before re-
jection. The solution containing the morphine crystals is to be brought
upon the double filter in the usual manner, and when this has drained, the
remaining crystals in the beaker and flask are to be transferred to the filter
by aid of a saturated aqueous solution of morphine, with which the crystals
are to be thoroughly washed. When drained, the filters containing the
crystals are to be carefully removed from the funnel, pressed with caution
between folds of filter-paper, and dried at a temperature not exceeding
60

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